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Index
Cover image Title page Table of Contents Copyright Acknowledgements Chapter 1. Introduction Chapter 2. Safety
General Laboratory Procedure Personal Safety Equipment REFERENCES
Chapter 3. Common Analytical Techniques for Nanoscale Materials
Principles of Electron Microscopy Transmission Electron Microscopy Sample Preparation for TEM Scanning Electron Microscopy Sample Preparation in SEM Scanning Tunnelling Microscopy Atomic Force Microscopy Powder X-ray Diffraction UV-visible Spectroscopy Dynamic Light Scattering and Zeta Potential Measurement BET Surface Area Measurement REFERENCES
Chapter 4. Chemical Techniques
The Sol–Gel Process Silica Sodium Silicate Silica Nanoparticles Titania Nanoparticles Making Titania Nanoparticles using Titanium Tetrachloride as a Precursor Preparing Sub 4 nm Nanoparticles Using an Alkoxide Titanium Precursor Making Larger Titania Spheres from Titania Glycolates Making Black Titania Nanoparticles Coating Nanomaterials Using the Sol Gel Method Silica Coating a Gold Colloid Glass Coating an Organic Crystal Template How to Coat a Virus Template with Silica How to Coat Carbon Nanotubes in Silica and Other Oxides using the Sol Gel Process Coating MultiWalled Carbon Nanotubes in Zirconia Using Sol Gel Dip Coating to Form Thin Films, Thin Porous Films and Replicas Dip Coating Dip Coating a Glass Film Making a Dip Coating Chamber Making a Cubic Phase in a Dip coated Silica Film Using Cetyltrimethylammonium Bromide Dip Coating to Form a Doped Tin Oxide Film Dip Coating to Form an Anatase Phase Titania Film Replication of Oddly Shaped Morphologies Using Sol Gel Techniques Replicating Pollen with Titania Using a Sol Gel Approach Making a Cuttlefish Bone Replica Making a Superconducting Cuttlebone Mesoporous Inorganic Powders Making a Porous Aluminosilicate Zeolite MCM-41 An Alkoxide Approach to MCM-41 Preparation An Alkoxide Approach to MCM-48 Preparation Making a Monolithic Silica Structure from Non-ionic Surfactants using a Diol Based Silica Precursor Aerogels and Supercritical Drying Applications of Aerogels Making Silica Aerogel Monoliths Troubleshooting Cloudiness Spherical or Coin-Shaped Bubbles Stiction Wavy Surfaces Adjustable Parameters and Alternative Methods Recipe for Making Hydrophobic Silica Aerogel Monoliths Monoliths and Glasses Containing Functional Biological Materials Making a Glass Containing Yeast Making a Microtiter Plate Diagnostic for Glucose, Galactose, Lactose and Lactate Making an Optical Thick Film Sensor Bioglass for the Detection of D-glucose-6-Phosphate Growing Zinc Oxide Nanorods Making Seed Layers for the Hydrothermal Growth of Zinc Oxide Nanorods Thermal Decomposition of Zinc Acetate To Seed a Substrate Layer Using a Colloid Hydrothermal Growth of Zinc Oxide Nanorods Cadmium Sulfide, Selenide and Telluride Quantum Dots A Quick Water Based Method for the Preparation of Cadmium Sulfide Nanoparticles Coating the TMV Virus with Cadmium Sulfide Preparing Cadmium Selenide or Cadmium Telluride Quantum Dots with Well Defined Size Control Making Zinc Sulfide Coated Cadmium Selenide Nanoparticles Stable in Water Suface Modification of Cadmium Selenide Nanoparticles for use as Fluorescent Labels and Probes Functionalising the Quantum Dots with Transferrin Tagging the Mercaptoacetic Acid Stabilised Zns Coated CdSe Nanoparticles with Streptavidin so they can be Used for Target Specific Labelling Cadmium Selenide Nanorods Making Gold and Silver Colloids Making an Aqueous Gold Colloid Using the Frens Method Making an Oil Stable Alkanethiol Coated Gold Colloid Using the Brust Method How to Make Gold Nanorods How to Make Triangular Gold Nanoparticles Using Plasmon Resonance in Gold Colloids as a Colorimetric Test for Various Molecules A Quick Demonstration of Changing Colour and Colloid Stability with Varying Salt Concentration and PH DNA Based Gold Assemblies and Aptamer Colorimetric Tests Silver Nanoparticles and Structures Making a Basic Silver Colloid by Reduction with Citric Acid Preparation of Fluorescent Silver Nanoclusters Making Silver Nanocubes and Rods Using the Polyol Process A Hydrothermal Water Based Method for Preparing Silver Nanocubes Ferrofluids Magnetite Colloid Stabilised by Tetramethyl- or Tertabutylammonium Hydroxides Magnetite Colloids Stabilised by a Biopolymer Making a Polyol Stabilised Magnetite Colloid Making Stable Ferrofluids in Non Polar Solvents Making a Glass Coated Maghemite Colloid Allotropes of Carbon The Buckminsterfullerene Carbon Nanotubes Graphene and Graphene Oxide Metal Organic Frameworks Cobalt Bipyridyl Polymer Prussian Blue Analogues, a Molecular Magnet Framework Microemulsion Production of Cubic Prussian Blue Particles Making a MOF With Large Pores REFERENCES
Chapter 5. Physical Techniques
Chemical Vapour Deposition CVD Using Silica or Titania Precursors Atomic Layer Deposition Photolithography Patterning Clean Room Practices for Microfabrication Cleaning the Substrate Resolution and Pattern Transfer onto a Photoresist layer Reactive Ion Etching (RIE) Chemical Etching with KOH Solution Soft Lithography, Pattern Replication and Contact Printing Casting a Negative Mould Using PDMS Patterning a Self-Assembled Monolayer onto a Gold Substrate Using a PDMS Stamp Making a Microfluidic Device Using Soft Lithographic Templating Making Wire Tips for Scanning Tunnelling Microscopy Making a Platinum/Iridium STM Tip Making a Tungsten STM Tip by Wet Electrochemical Etching Etching a tungsten tip using alternating current in a beaker Etching Tungsten Tips Using Direct Current Direct Current Etching of Tungsten Tips Using the ‘Loop’ Method Sticking a Particle Onto a Scanning Probe Microscopy Tip Electrospinning Fibres from Polymeric Solutions Making a Solar Cell Using Titanium Dioxide Nanoparticles and Conductive Glass Electrodes Making a Conductive Glass Electrode REFERENCES
Chapter 6. Biological Nanotechnology
Cloning and Gene Expression to Produce Proteins in Escherichia Coli Inserting a Gene into a Plasmid Vector Plasmid Modification – Using Restriction Enzymes Plasmid Modification for Gene Excision – Primers and PCR Cutting the GFP Gene from the Subcloned Plasmid and Transferring it to the pET-45b Plasmid Vector Using Restriction Enzymes Transformation and Cloning Growing up a Colony and Triggering Expression of the GFP Protein Purification of His6 Tagged Protein Sodium Dodecyl Sulphate – Poly(acrylamide) Gel Electrophoeresis (SDS-PAGE) for Separating Proteins Transformation of Yeast DNA Origami Designing a DNA Origami Shape Using a Program Making a DNA Scaffold from M13 Bacteriophage Running the Self-Assembly Using the Single-Stranded DNA and the Staples Purification and Analysis of DNA Products Agarose Gel Electrophoresis for Checking the DNA Product from a Polymerase Chain Reaction (PCR) Keeping Bacteria Long Term in a Glycerol Stock Testing the Minimum Inhibitory Concentration of an Antibiotic REFERENCES
Index
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